TABLE 1. ¹H NMR DATA Data taken from Gottlieb, H. E., Kotlyar, V., and Nudelman, A.; NMR Chemical Shifts of Common Laboratory Solvents as Trace Impurities, J. Org. Chem 1997, 62, 7512-7515

	Proton	mult	CDCL3	(CD3)2CO	(CD3)2SO	C6D6	CD3 CN		CD3OD	D2O
solvent residual peak			7.26	2.05	2.50	7.16		1.94	3.31	4.79
H20		s	1.56	2.84a	3.33a	0.40		2.13	4.87
acetic acid	CH3	s	2.10	1.96	1.91	1.55		1.96	1.99	2.08
acetone	CH3	s	2.17	2.09	2.09	1.55		2.08	2.15	2.22
acetonitrile	CH3	s	2.10	2.05	2.07	1.55		1.96	2.03	2.06
benzene	CH	s	7.36	7.36	7.37	7.15		7.37	7.33
tert-butyl methyl alcohol	CH3	s	1.28	1.18	1.11	1.05		1.16	1.40	1.24
	OHc	s			4.19	1.55		2.18
tert-butyl methyl ether	CCH3	s	1.19	1.13	1.11	1.07		1.14	1.15	1.21
	OCH3	s	3.22	3.13	3.08	3.04		3.13	3.20	3.22
BHTb	ArH	s	6.98	6.96	6.87	7.05		6.97	6.92
	OHc	s	5.01		6.65	4.79		5.20
	ArCH3	s	2.27	2.22	2.18	2.24		2.22	2.21
	ArC(CH3)3	s	1.43	1.41	1.36	1.38		1.39	1.40
chloroform	CH	s	7.26	8.02	8.32	6.15		7.58	7.90
cyclohexane	CH2	s	1.43	1.43	1.40	1.40		1.44	1.45
1,2-dichloroethane	CH2	s	3.73	3.87	3.90	2.90		3.81	3.78
dichloromethane	CH2	s	5.30	5.63	5.76	4.27		5.44	5.49
diethyl ether	CH3	t,7	1.21	1.11	1.09	1.11		1.12	1.18	1.17
	CH2	q,7	3.48	3.41	3.38	3.26		3.42	3.49	3.56
diglyme	CH2	m	3.65	3.56	3.51	3.46		3.53	3.61	3.67
	CH2	m	3.57	3.47	3.38	3.34		3.45	3.58	3.61
	OCH3	s	3.39	3.28	3.24	3.11		3.29	3.35	3.37
1,2-dimethoxyethane	CH3	s	3.40	3.28	3.24	3.12		3.28	3.35	3.37
	CH2	s	3.55	3.46	3.43	3.33		3.45	3.52	3.60
dimethylacetamide	CH3CO	s	2.09	1.97	1.96	1.60		1.97	2.07	2.08
	NCH3	s	3.02	3.00	2.94	2.57		2.96	3.31	3.06
	NCH3	s	2.94	2.83	2.78	2.05		2.83	2.92	2.90
dimethylformanamide	CH	s	8.02	7.96	7.95	7.63		7.92	7.97	7.92
	CH3	s	2.96	2.94	2.89	2.36		2.89	2.99	3.01
	CH3	s	2.88	2.78	2.73	1.86		2.77	2.86	2.85
dimethyl sulfoxide	CH3	s	2.62	2.52	2.54	1.68		2.50	2.65	2.71
dioxane	CH2	s	3.71	3.59	3.57	3.35		3.60	3.66	3.75
ethanol	CH3	t, 7	1.25	1.12	1.06	0.96		1.12	1.19	1.17
	CH2	q, 7d	3.72	3.57	3.44	3.34		3.54	3.60	3.65
	OH	sc,d	1.32	3.39	4.63			2.47
ethyl acetate	CH3CO	s	2.05	1.97	1.99	1.65		1.97	2.01	2.07
	CH2CH3	q, 7	4.12	4.05	4.03	3.89		4.06	4.09	4.14
	CH2CH3	t, 7	1.26	1.20	1.17	0.92		1.20	1.24	1.24
ethyl methyl ketone	CH3CO	s	2.14	2.07	2.07	1.58		2.06	2.12	2.19
	CH2CH3	q, 7	2.46	2.45	2.43	1.81		2.43	2.50	3.18
	CH2CH3	t, 7	1.06	0.96	0.91	0.85		0.96	1.01	1.26
ethylene glycol	CH	se	3.76	3.28	3.34	3.41		3.51	3.59	3.65
"grease"f	CH3	m	0.86	0.87		0.92		0.86	0.88
	CH2	br s	1.26	1.29		1.36		1.27	1.29
n-hexane	CH3	t	0.88	0.88	0.86	0.89		0.89	0.90
	CH2	m	1.26	1.28	1.25	1.24		1.28	1.29
HMPAg	CH3	d, 9.5	2.59	2.65	2.53	2.40		2.57	2.64	2.61
methanol	CH3	sh	3.49	3.31	3.16	3.07		3.28	3.34	3.34
	OH	sc,h	1.09	3.12	4.01			2.16
nitromethane	CH3	s	4.33	4.43	4.42	2.94		4.31	4.34	4.40
n-pentane	CH3	t, 7	0.88	0.88	0.86	0.87		0.89	0.90
	CH2	m	1.27	1.27	1.27	1.23		1.29	1.29
2-propanol	CH3	d, 6	1.22	1.10	1.04	0.95		1.09	1.50	1.17
	CH	sep, 6	4.04	3.90	3.78	3.67		3.87	3.92	4.02
pyridine	CH(2)	m	8.62	8.58	8.58	8.53		8.57	8.53	8.52
	CH(3)	m	7.29	7.35	7.39	6.66		7.33	7.44	7.45
	CH(4)	m	7.68	7.76	7.79	6.98		7.73	7.85	7.87
silicone greasei	CH3	s	0.07	0.13		0.29		0.08	0.10
tetrahydrofuran	CH2	m	1.85	1.79	1.76	1.40		1.80	1.87	1.88
	CH2O	m	3.76	3.63	3.60	3.57		3.64	3.71	3.74
toluene	CH3	s	2.36	2.32	2.30	2.11		2.33	2.32
	CH(o / p)	m	7.17	7.1-7.2	7.18	7.02		7.1-7.3	7.16
	CH(m)	m	7.25	7.1-7.2	7.25	7.13		7.1-7.3	7.16
triethylamine	CH3	t,7	1.03	0.96	0.93	0.96		0.96	1.05	0.99
	CH2	q,7	2.53	2.45	2.43	2.40		2.45	2.58	2.57

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